Solvent-controlled selective synthesis of biphenols and quinones via oxidative coupling of phenols.
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2017
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Abstract
A regioselective synthesis of unsymmetrical and symmetrical biphenols and binaphthols via oxidative coupling of phenols or naphthols in the presence of KSO in CFCOOH under ambient conditions is described. Interestingly, the 1 : 1 ratio of HO and CHCN solvent mixtures at 80 °C instead of CFCOOH provided substituted unsymmetrical quinones. A gram-scale synthesis of biphenols and binaphthols was demonstrated.
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| Authors | More, Nagnath Yadav;Jeganmohan, Masilamani; |
| Journal | Chemical communications (Cambridge, England) |
| Year | 2017 |
| DOI |
10.1039/c7cc04829g
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