Chiroptical Spectroscopy of Mechanically Fragile Single Crystals Without Sample Degradation

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ID: 315292
2026
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Abstract
Abstract This study presents a nondestructive method to evaluate solid-state circular dichroism (CD) and circularly polarized luminescence (CPL) without matrix dispersion. Chiral co-crystals of tartaric or malic acid with 1-aminopyrene were used as models. Conventional matrix preparation damaged the malic acid co-crystal, eliminating its CD signal. Using an in situ diffuse-reflectance CD spectrometer and CPL spectrometer with polarization analysis, we obtained artifact-free CD and CPL spectra without sample damage, enabling reliable chiroptical analysis of sensitive solid-state materials.
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Authors Misaki Rikioka, Hatsune Nakayama, C. Kachi-Terajima, Takunori Harada
Journal phytochemistry letters
Year 2026
DOI
10.1093/chemle/upag101
URL
https://doi.org/10.1093/chemle/upag101
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