Iodine titration voltameter
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Abstract
THE rapidity, accuracy and sharpness of the end reaction of several of the methods of.volumetlie analysis, particularly of the iodometric 111et11ods,have suggested the possibility of apply111g them to the volta111ete1'.Arather extensive investigation of quantitative electrolytic oxidation and 1eduction methods, with this aim in View, has resulted in the evolution of a titration voltameter the accuracy of which may be depended upon to about one part in ten thousand.The advantages in point of 1111111ip111atio11 and time required, as well as its applicability to a greater range of current density, Will, in the writer's opinion, make it of service in many investigations.The basis of the method is the electrolysis of potassium iodide and the titration of the liberated iodine by sodium thiosulphate.Herroun'x' first suggested the use of iodine in this ' connection.He electrolyzed zinc iodide between a platinum anode and zinc cathode in a 1:1eake1'; but gives the results of only one determination and leaves the method in an impracticable to1111DanneehL repmts four eOmparative tests of Herr'soun zinc iodide volta111ete1111 se11es Witha silve1'volta111ete1.The 1esults show a difference of between +O'2'7 per cent and -1 per cent.His b111ette readings were made to only the 11ea1est O lcc, and the total quantity of thiosulphate Was s111all'va1y111o' 1101117 to 34:cc.The work of Da1111eel,as well as that of Kistiakowskyi 011 a silver titration volta111ete1',see111s neve1 to have found its way * Phil.Mag.
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|---|---|
| Authors | D. Albert Kreider |
| Journal | american journal of science |
| Year | 1905 |
| DOI |
10.2475/ajs.s4-20.115.1
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| URL | |
| Keywords | Keywords not found |
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