Photoinduced synthesis of fluorinated dibenz[b,e]azepines via radical triggered cyclization.

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ID: 26450
2019
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Ranked #119 of 184 articles by views in Chemical communications (Cambridge, England)

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Abstract
A simple, mild and efficient approach to access fluorinated dibenz[b,e]azepines via visible-light photoredox catalysis is presented. Inexpensive and commercially available fluoroalkyl anhydrides in concert with pyridine N-oxide are employed as the source of the fluoroalkyl radicals. A one-pot process involving the trifluoroacetylation of unprotected secondary benzyl amines followed by radical cyclization could also afford the desired fluorinated dibenz[b,e]azepines.
Reference Key
qi2019photoinducedchemical Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Qi, Xu-Kuan;Zhang, Hong;Pan, Zi-Tong;Liang, Rong-Bin;Zhu, Can-Ming;Li, Jing-Hong;Tong, Qing-Xiao;Gao, Xue-Wang;Wu, Li-Zhu;Zhong, Jian-Ji;
Journal Chemical communications (Cambridge, England)
Year 2019
DOI
10.1039/c9cc04977k
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