copper-based nanoparticles prepared from copper (ii) acetate bipyridine complex
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ID: 250594
2016
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Abstract
We report the synthesis of CuO, Cu/Cu2O and Cu2O/CuO nanoparticles (NPs) from
the single copper (II) acetate bipyridine complex by three different
methods:microwave-assisted, solvothermal and borohydride. Presence of
bipyridine ligand in the copper complex would impose no need in additional
stabilization during synthesis. The phases of formed NPs were identified by
X-ray diffraction. CuO NPs of ~11 nm were obtained via solvothermal synthesis
from alkaline solution at 160°C. The Cu/Cu2O NPs of ~80 nm were produced via
microwave-assisted polyol procedure at 185-200°C, where ethylene glycol can
play a triple role as a solvent, a reducing agent and a surfactant. The
Cu2O/CuO NPs of ~16 nm were synthesized by a borohydride method at room
temperature. Interplanar spacing calculated from the selected-area electron
diffraction data confirmed the formation of Cu, CuO and Cu2O phases in
respective samples. All NPs are stable and can be used for various
applications including biomedicine.
| Reference Key |
a.2016journalcopper-based
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|---|---|
| Authors | ;Lastovina Tatiana A.;Budnyk Andriy P.;Khaishbashev Gevorg A.;Kudryavtsev Egor A.;Soldatov Alexander V. |
| Journal | meditsinskaia radiologiia |
| Year | 2016 |
| DOI |
10.2298/JSC151211036L
|
| URL | |
| Keywords | Keywords not found |
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