Yolk-Shell Polystyrene@Microporous Organic Network: A Smart Template with Thermally Disassemblable Yolk To Engineer Hollow MoS/C Composites for High-Performance Supercapacitors.

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ID: 24890
2017
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Abstract
Yolk-shell-type polystyrene@microporous organic network (Y-PS@MON) materials were prepared by the Sonogashira coupling of tetra(4-ethynylphenyl)methane and 1,4-diiodobenzene on the surface of PS@SiO and by the etching of SiO. The diameter of PS yolk spheres and the thickness of MON shells were 150 and ∼10 nm, respectively. The thickness of the void space between the PS yolk and the MON shell was ∼30 nm. Y-PS@MONs were used as templates for the synthesis of MoS/C composite materials. Because of the microporosity of the MON shells and the void space between the yolk and the shell, MoS precursor compounds were efficiently incorporated into Y-PS@MONs. The heat treatment under argon resulted in the formation of hollow MoS/C composites. The contents of MoS in the composites were systematically controlled by changing the amounts of precursor. MoS/C with 58 wt % of MoS showed the best energy storage performance with a capacitance of 418 F/g at a 0.5 A/g current density as an electrode material of a coin cell supercapacitor, which is attributable to its hollow structure, high surface area, and the good distribution of the sliced MoS in the carbon matrix. Also, the MoS/C-58 composite showed excellent retention of capacitances during 5000 cycles.
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lee2017yolkshellacs Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Lee, Hyunjae;Choi, Jaewon;Myung, Yoon;Lee, Sang Moon;Kim, Hae Jin;Ko, Yoon-Joo;Yang, MinHo;Son, Seung Uk;
Journal ACS omega
Year 2017
DOI
10.1021/acsomega.7b01426
URL
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