ethyl 2,6-dimethoxybenzoate: synthesis, spectroscopic and x-ray crystallographic analysis
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ID: 236942
2012
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Abstract
The acid catalyzed esterification of 2,6-dimethoxybenzoic acid (1) in the presence of absolute ethanol afforded ethyl 2, 6-dimethoxybenzoate (2). The structure of the resulting compound was supported by spectroscopic data and unambiguously confirmed by single crystal X-ray diffraction studies. The title compound crystallized in the triclinic space group P ī with unit cell parameters a = 8.5518(3) Å, b = 10.8826(8) Å, c = 11.9939(6) Å, α = 101.273(5)°, β = 98.287(3)°, γ = 94.092(4)°, V = 1077.54(10) Å3, Z = 4, Dc = 1.296 Mg/m3, F(000) = 448 and μ = 0.098 mm−1. Compound (2) crystallizes with two molecules in the asymmetric unit with similar conformations.
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white2012crystalsethyl
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| Authors | ;Jonathan M. White;Aliya Ibrar;Imtiaz Khan |
| Journal | turk kardiyoloji dernegi arsivi |
| Year | 2012 |
| DOI |
10.3390/cryst2020521
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