crystal structure of chloridobis[(1,2,5,6-η)-cycloocta-1,5-diene]iridium(i)

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ID: 227648
2017
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Abstract
The title complex, [IrCl(C8H12)2], was synthesized directly from the reaction of IrCl3·3H2O with a large excess of cod (cod = cycloocta-1,5-diene) in alcoholic solvent. Large yellow needles were obtained by the slow cooling of a hot solution. Based on the positions of the chloride ligand and the mid-points of the four C=C bonds, the molecule adopts a five-coordinate geometry that is midway between square pyramidal and trigonal bipyramidal. The material crystallizes in the orthorhombic space group Pbca with one molecule per asymmetric unit in a general position and shows no significant intermolecular interactions. Individual molecules are aligned along [010], and these rows form a pseudo-hexagonal packing arrangement.
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rahman2017actacrystal Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors A. K. Fazlur Rahman, Miles Wilklow-Marnell, William W. Brennessel, William D. Jones
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Journal Disability and rehabilitation
Year 2017
DOI
10.1107/S2056989017000809
URL
http://scripts.iucr.org/cgi-bin/paper?S2056989017000809
Keywords
1 crystal structure

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