crystal structure of disodium dicobalt(ii) iron(iii) tris(orthophosphate) with an alluaudite-like structure
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ID: 195294
2015
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Abstract
The title compound, Na2Co2Fe(PO4)3, was synthesized by a solid-state reaction. This new stoichiometric phase crystallizes in an alluaudite-like structure. In this structure, all atoms are in general positions except for four atoms which are located at the special positions of the C2/c space group. One Co atom, one P and one Na atom are all located on Wyckoff position 4e (2), while the second Na atom is located on an inversion centre 4a (-1). The other Co and Fe atoms occupy a general position with a statistical distribution. The open framework results from [(Co,Fe)2O10] units of edge-sharing [(Co,Fe)O6] octahedra, which alternate with [CoO6] octahedra that form infinite chains running along the [10-1] direction. These chains are linked together through PO4 tetrahedra by the sharing of vertices so as to build layers perpendicular to [010]. The three-dimensional framework is accomplished by the stacking of these layers, leading to the formation of two types of tunnels parallel to [010] in which the Na+ cations are located, each cation being surrounded by eight O atoms.
| Reference Key |
bouraima2015actacrystal
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| Authors | ;Adam Bouraima;Abderrazzak Assani;Mohamed Saadi;Thomas Makani;Lahcen El Ammari |
| Journal | Disability and rehabilitation |
| Year | 2015 |
| DOI |
10.1107/S2056989015007926
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