synthesis, crystal structure of a novel mn complex with nicotinoyl-glycine

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ID: 183924
2016
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Abstract
A novel manganese complex, C16H26MnN4O12, was synthesized by the reaction of nicotinoyl-glycine and NaOH in an ethanol/water solution and structurally characterized by elemental analysis, UV-vis spectrum, IR spectrum and single-crystal X-ray diffraction analysis. The crystal of the complex belongs to the triclinic space group P1 with a = 7.8192(16) Å, b = 8.8800(18) Å, c = 9.0142(18) Å, α = 83.14(3)°, β = 65.27(3)°, γ = 81.67(3)°, V = 516.3(2) Å3, Z = 1, Dx = 1.542 mg·m−3, μ = 0.66 mm−1, F(000) = 271, and final R1 = 0.0381, ωR2 = 0.0964. The nicotinoyl-glycine ligand acts as a bridging ligand to connect the manganese ions by the hydrogen interactions; thus, the complex expands into a 3D supramolecular net structure.
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wang2016crystalssynthesis, Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Xin Wang, Biqing Chen, Min He
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Journal turk kardiyoloji dernegi arsivi
Year 2016
DOI
10.3390/cryst7010003
URL
http://www.mdpi.com/2073-4352/7/1/3
Keywords
synthesis manganese complex crystal structurecrystallography nicotinoyl-glycine

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