crystal structure of an organic–inorganic supramolecular salt based on a 4,4′-methylenebis(3,5-dimethyl-1h-pyrazol-2-ium) cation and a β-octamolybdate anion
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ID: 180758
2016
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Abstract
The asymmetric unit of the title compound, bis[4,4′-methylenebis(3,5-dimethyl-1H-pyrazol-2-ium)] β-octamolybdate, (C11H18N4)2[Mo8O26] or (H4mbdpz)2[Mo8O26], is composed of an H4mbdpz2+ cation and half of the β-octamolybdate anion which is completed by inversion symmetry. The organic molecular units are engaged in a series of N—H...O hydrogen bonds with neighbouring anions, with N...O distances and N—H...O angles in the ranges 2.730 (2)–2.941 (2) Å and 122–166°, respectively. These interactions lead to the formation of a supramolecular two-dimensional network parallel to the (010) plane.
| Reference Key |
amarante2016actacrystal
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| Authors | ;Tatiana R. Amarante;Isabel S. Gonçalves;Filipe A. Almeida Paz |
| Journal | Disability and rehabilitation |
| Year | 2016 |
| DOI |
10.1107/S2056989015024524
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