comparação de metodologias para a determinação do ph e do ponto de congelamento do leite bovino cru sob diferentes características de conservação comparison of methodologies for the determination of ph and freezing point in raw bovine milk under different conservation characteristics

Clicks: 154
ID: 175196
2011
Free PDF
Article Quality & Performance Metrics
Overall Quality
Not rated
Combines reader engagement with the AI quality analysis. This article has not been analysed, so there is no overall score — reader engagement is measured and shown alongside.
AI Quality Assessment
Not analyzed
Readership in this journal
Steady

Ranked #224 of 235 articles by views in european journal of lipid science and technology

Most read Least read

Bar heights use a square-root scale. Only the 120 most-read articles are drawn; the journal has 235 in total.

Mint this article as an NFT
Not yet minted

Create a permanent, verifiable on-chain record of this article on the Scimatic Network. The NFT is held in your Journament account, and you can withdraw it to your own wallet at any time.

5 SUSD one-off · no wallet required
Sign in to mint
Abstract
Objetivou-se comparar metodologias de referência com a espectroscopia de infravermelho com transformada de Fourier para análises do pH e do ponto de congelamento sob diferentes condições de conservação em amostras de leite bovino cru. Foram coletadas amostras de leite de tanques de expansão em 57 propriedades. Cada amostra foi subdividida em 45 frascos (40 mL), que foram distribuídos de acordo com a temperatura de armazenamento (-20; 7 e 25ºC), a idade da amostra (0, 3, 6 e 9 dias) e os níveis de adição de água (0, 2, 4 e 6%). Foi adicionado bronopol a 44 frascos e um foi mantido sem adição do conservante para controle. O pH e o ponto de congelamento foram determinados pela metodologia de referência (potenciômetro e crioscópio eletrônico, respectivamente) e pela metodologia alternativa por meio do equipamento MilkoScanTM FT+. Os resultados obtidos em cada metodologia nas diferentes condições de conservação das amostras foram avaliados por análise de variância e comparação de médias. A análise de regressão linear foi realizada para avaliar as metodologias (referência e alternativa) quanto aos resultados do ponto de congelamento em função da idade da amostra. O bronopol não alterou as médias de pH, porém reduziu o ponto de congelamento. Foram calculados fatores de correção para eliminar esse efeito nos resultados do ponto de congelamento. As médias de pH em amostras com três dias, mantidas a -20 e 25ºC foram mais baixas que as amostras a 7ºC. A idade da amostra influenciou os resultados de pH quando as amostras foram submetidas a 25ºC. O aumento da temperatura de armazenamento para 25ºC reduziu as médias do ponto de congelamento em amostras sem adição de água e com nove dias de armazenagem. O aumento na idade da amostra a -20 e 7ºC não tem efeito sobre médias do ponto de congelamento. Há forte correlação entre as metodologias em função da idade da amostra para o ponto de congelamento.
The objective of this work was to compare reference methodologies to Fourier transform infrared spectroscopy for analysis of pH and freezing point (FP) under different storage conditions on samples of raw bovine milk. Milk samples were collected from bulk tank milk on 57 farms. Each sample was subdivided into 45 vials (40 mL) which were distributed according to storage temperature (-20ºC, 7ºC and 25ºC), age of the sample (0, 3, 6 and 9 days) and levels of water addition (0, 2, 4 and 6%). Bronopol was added into 44 flasks and one was maintained without addition of preservative for control. Frozen point and pH were determined by the standard methods (thermistor cryoscope and potentiometer, respectively) and by the alternative methodology by using MilkoScanTM FT+. The results from each method, at different conditions of conservation of the samples, were evaluated by analysis of variance and comparison of means. The linear regression analysis was performed to evaluate the methodologies (reference and alternative) for results of the frozen point in function of the age of the sample. Bronopol did not alter pH means, but it reduced frozen point. Correction factors were calculated to eliminate this effect on the results of the frozen point. Means of pH in three-day samples, kept at -20ºC and 25ºC were lower than the samples at 7ºC. The age of the samples affected the results of pH when they were submitted to 25ºC. The increase of storage temperature to 25ºC reduced means of frozen point in samples without addition of water and at nine days of storage. The increase in age of sample at -20ºC and 7ºC does not affect means of frozen point. There is a strong correlation among methodologies in function of age of the sample for frozen point.
Reference Key
arajo2011revistacomparao Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Viviane Maia de Araújo, Laerte Dagher Cassoli, Aline Zampar, Augusto Cesar Lima da Silva, Carlos Tadeu dos Santos Dias, Paulo Fernando Machado
Are you one of these authors? Claim your profile
Journal european journal of lipid science and technology
Year 2011
DOI
10.1590/S1516-35982011000700030
URL
http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1516-35982011000700030
Keywords Keywords not found

Citations

No citations found. To add a citation, contact the admin at info@scimatic.org

Comments

No comments yet. Be the first to comment on this article.