crystal structure of tris(μ-bis{4-[(pyridin-2-ylmethylidene)amino]phenyl}methane-κ4n,n′:n′′,n′′′)dizinc tetrakis(tetrafluoridoborate) acetonitrile trisolvate
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ID: 174876
2015
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Abstract
The asymmetric unit of the title compound, [Zn2(C25H20N4)3](BF4)4·3CH3CN, consists of one dinuclear ZnII complex cation with a triple-helical [Zn2L3]4+ motif (L is bis{4-[(pyridin-2-ylmethylidene)amino]phenyl}methane), four BF4− anions and three CH3CN solvent molecules. The Zn...Zn separation is 11.3893 (14) Å and the ligands wrap around the two ZnII atoms, forming a triple helix as defined by the Zn—N—N—Zn torsion angles of 104.05 (18), 99.06 (19) and 101.40 (19)°. The Zn—N(pyridyl) distances in the octahedral ZnN6 coordination sphere are in the range 2.128 (5)–2.190 (5) Å and the Zn—N(imine) distances are in the range 2.157 (5)–2.277 (5) Å.
| Reference Key |
alexandru2015actacrystal
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|---|---|
| Authors | ;Maria-Gabriela Alexandru;Florina Dumitru |
| Journal | Disability and rehabilitation |
| Year | 2015 |
| DOI |
10.1107/S205698901502455X
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