synthesis and crystal structure of a zn(ii)-based mof bearing neutral n-donor linker and sif62− anion

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ID: 174021
2018
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Abstract
A novel three-dimensional two-fold interpenetrated bi-porous metal-organic framework IPM-325 (IPM: IISER Pune Materials) having pcu topology was synthesized at room temperature. Single crystal X-ray diffraction (SC-XRD) study revealed that the compound crystallizes in monoclinic lattice with molecular formula {[Zn(L)2 (SiF6)] (CH2Cl2) xG}n where G = Guests). All metal centers were found to have octahedral geometry. From single crystal analysis it can be inferred that SiF62− anion play a vital role in extending the dimensionality of the framework by bridging between two metal centers. Interestingly, IPM-325 exhibited two-step structural transformation maintaining the crystallinity of the framework as characterized by powder X-ray diffraction (PXRD).
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manna2018crystalssynthesis Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Biplab Manna, Shivani Sharma, Sujit K. Ghosh
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Journal turk kardiyoloji dernegi arsivi
Year 2018
DOI
10.3390/cryst8010037
URL
http://www.mdpi.com/2073-4352/8/1/37
Keywords
metal-organic framework

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