crystal structure of bis(μ2-4-bromo-2-[({2-[({2-[(5-bromo-2-oxidobenzylidene)amino]ethyl}sulfanyl)sulfonyl]ethyl}imino)methyl]phenolato)dicopper(ii) dimethylformamide disolvate
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ID: 166950
2017
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Abstract
The title dinuclear copper(II) complex [Cu2(C18H16Br2N2O4S2)2] was prepared by direct synthesis of a dianionic Schiff base derived from 5-bromosalicylaldehyde and cysteamine. The discrete molecules lie across inversion centers and crystallize with two dimethylformamide (DMF) molecules of crystallization. The unique CuII ion is four-coordinated by two tetradentate Schiff base ligands in a distorted square-planar N2O2 environment. In the crystal, short intermolecular S...Br contacts, weak C—H...O hydrogen bonds and intra- and intermolecular π–π stacking interactions between rings of the ligand link the components into a two-dimensional network parallel to (010).
| Reference Key |
rusanova2017actacrystal
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|---|---|
| Authors | ;Julia A. Rusanova;Dmytro Bederak |
| Journal | Disability and rehabilitation |
| Year | 2017 |
| DOI |
10.1107/S2056989017015584
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