the thermal decomposition of the pyridine saccharinates of co, ni and cu: a correlation of the structural and the infrared data
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ID: 165931
1999
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Abstract
In order to investigate the differences in the stability of the isomorphous pyridine saccharinates [Co(H2O)4(C5H5N)2](C7H4NO3S)2·H2O and [Ni(H2O)4(C5H5N)2[ (C7H4NO3S)2·4H2O, their thermal behavior (TG, DTG and DTA curves) from ambient temperature up to 1000°C in a static air atmosphere was studied. For comparative purposes, the thermoanalytical curves of [Cu(H2O)(C5H5N)2(C7H4NO3S)2] were recorded as well. The decomposition pathways and the stability of the compounds are interpreted in the terms of the structural data. A possible mechanism for the decomposition of the saccharinato ion/ligand in an oxidizing atmosphere is proposed. The infrared spectral characteristics of the complexes are also discussed.
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| Authors | ;BOYAN BOYANOV;VERA JORDANOVSKA;GLIGOR JOVANOVSKI;PANCE NAUMOV |
| Journal | meditsinskaia radiologiia |
| Year | 1999 |
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