An Energetic Triazolo-1,2,4-Triazine and its N-Oxide.

Clicks: 217
ID: 16046
2016
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Abstract
The reaction of 3-amino-5-nitro-1,2,4-triazole with nitrous acid produces the corresponding diazonium salt. When the diazonium salt is treated with nitroacetonitrile, a subsequent condensation and cyclization reaction occurres to produced 4-amino-3,7-dinitrotriazolo-[5,1-c][1,2,4] triazine (DPX-26). X-ray crystallographic analysis shows that the DPX-26 has a density of 1.86 g cm , while it is calculated to have a heat of formation of 398.3 kJ mol . DPX-26 is predicted to approach the explosive performance of RDX but displays significantly better safety properties. Oxidation of DPX-26 using hypofluorous acid produces 4-amino-3,7-dinitrotriazolo-[5,1-c][1,2,4] triazine 4-oxide (DPX-27), which is also predicted to be a high-performance material with enhanced safety properties.
Reference Key
piercey2016anangewandte Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Piercey, Davin G;Chavez, David E;Scott, Brian L;Imler, Greg H;Parrish, Damon A;
Journal angewandte chemie (international ed in english)
Year 2016
DOI
10.1002/anie.201608723
URL
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