synthesis of substituted thioureas and their sulfur heterocyclic systems of p-amino salicylic acid as antimycobacterial agents

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ID: 154791
2013
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Abstract
A series of new N,N′-substituted thioureas (2, 6, and 8) and their sulfur heterocycles as thiobarbituric acids (3, 4, and 7), 2-thioxothiazoliodin-4-one (10), thiazolidin-4-one (11), 1,2,4-triazol-5-thione (14), and 1,3,4-thiadiazole (15) of p-Amino salicylic acid (PAS) have been synthesized from treatment with dithiocarbazinate (1, 5 and 12) followed by heterocyclization with dimethyl malonate, chloroacetic acid, and/or trifluoroacetic anhydride. The structures of the newly synthesized compounds were substantiated with IR, H1, and C13 NMR spectral data and elementary microanalyses. The in vitro antitubercular activity of synthesized compounds against M. tuberculosis strain H37Rv showed moderate-to-good activity.
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Authors ;Mohammed Saleh I. T. Makki;Reda M. Abdel-Rahman;Hassan M. Faidallah;Khalid Ali Khan
Journal british journal of psychology (london, england : 1953)
Year 2013
DOI
10.1155/2013/862463
URL
http://dx.doi.org/10.1155/2013/862463
Keywords
chemistry

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