the synthesis and molecular structure of 1-(3,4-dihydroxyphenethyl)-3-hydroxy-2-methylpyridin-4(1h)-one hydrochloride methanol solvate

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2013
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Abstract
A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; α = 73.566(2)°; β = 84.514(2)°; γ = 66.578(2)°. The asymmetric unit contains two molecules.
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Authors ;Andreas Decken;Christopher M. Vogels;L. Ross C. Barclay;Kate J. Sullivan;Dylan T. McLaughlin;Raymond Roy;Steven R. Hall;Stephen A. Westcott
Journal turk kardiyoloji dernegi arsivi
Year 2013
DOI
10.3390/cryst3020333
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