synthesis of batio3 from a mechanically activated baco3-tio2 system

Clicks: 138
ID: 139254
2008
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Abstract
In this article the solid state reaction of BaTiO3 formation from a mechanically activated BaCO3-TiO2 system has been investigated. An equimolar mixture of BaCO3 and TiO2 powders was activated in a planetary ball mill in a continual regime for 0, 30 and 90 min, pressed and thermally treated up to 1200oC. The effect of the milling and firing regime on the phase formation was investigated by the X-ray diffraction (XRD) method and differential thermal analysis (DTA). Deconvolution of the experimental DTA curve corresponding to the BaTiO3 synthesis process has been performed. The influence of the activation time on the change of characteristic temperature for each elementary step in the complete solid-state reaction of BaTiO3 formation, was analyzed. These results were correlated with the ones obtained by SEM characterization and by XRD analysis.
Reference Key
v.p.2008sciencesynthesis Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors ;Pavlović V.P.;Stojanović B.D.;Pavlović V.B.;Marinković-Stanojević Z.;Živković Lj.;Ristić M.M.
Journal european romantic review
Year 2008
DOI
10.2298/SOS0801021P
URL
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