crystal structure of [2-({2-[(2-azanidylbenzylidene)amino]benzylidene}amino)-4-chlorophenolato]nickel(ii)

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ID: 129943
2017
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Abstract
The title complex, [Ni(C20H14ClN3O)], with an asymmetrically chloride-appended Schiff base ligand has been synthesized and structurally characterized at 100 K. In the compound, the central nickel(II) ion has a square-planar coordination geometry with N3O donors of the π-conjugated tetradentate Schiff base ligand. In the crystal, the complexes are connected into an inversion dimer via an Ni...Ni interaction [3.1753 (5) Å] and a pair of π–π interactions [centroid–centroid distance = 3.8416 (16) Å]. The dimers are linked via a C—H...Cl hydrogen bond, forming a chain along the c-axis direction. The dimer chains interact with each other through π–π interactions [centroid–centroid distance = 3.8736 (16) Å], forming a layer expanding parallel to the ac plane.
Reference Key
kobayashi2017actacrystal Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors ;Fumiya Kobayashi;Atsushi Koga;Ryo Ohtani;Shinya Hayami;Masaaki Nakamura
Journal Disability and rehabilitation
Year 2017
DOI
10.1107/S2056989017004613
URL
http://scripts.iucr.org/cgi-bin/paper?S2056989017004613
Keywords
crystal structure nickel(ii) complex asymmetric structure

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