A Convenient One-Pot and Rapid Microwave-Assisted Synthesis of Biologically Active -Triazolo[3,4-b][1,3,4]Thiadiazine and -Triazolo[3,4-b][1,3,4]Thiadiazole Nanoarchitectonics.

Clicks: 223
ID: 64092
2020
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Abstract
A rapid and efficient one-pot protocol has been developed for the synthesis of s-triazolo[3,4-b][1,3,4]thiadiazine and s-triazolo[3,4-b][1,3,4]thiadiazole nanoarchitectonics through the reaction of s-triazoles with ketones and nitriles in acetic acid containing a catalytic amount of sulfuric acid under microwave irradiation in excellent yields. With this catalytic reaction, the cheap sulfuric acid as well as other acids were examined as catalysts and the highly toxic and irritating haloketones and halonitriles were avoided to form. The effects of microwave power, temperature, time, solvent and catalyst were examined. This method achieved a better performance; e.g., higher yields, shorter reaction time and easier work-up as compared to other conventional methods. Therefore, the proposed method will be readily applicable to the synthesis of biologically important compounds containing s-triazolo[3,4-b][1,3,4]thiadiazine and s-triazolo[3,4-b][1,3,4]thiadiazole framework.
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elmahdy2020ajournal Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors El-Mahdy, Ahmed F M;El-Sherief, Hassan A H;Hozien, Zeinab A;Kuo, Shiao-Wei;
Journal Journal of nanoscience and nanotechnology
Year 2020
DOI
10.1166/jnn.2020.17452
URL
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