In-Water Synthesis of 5-Thiolated 1,2,3-Triazoles From β-Thioenaminones by Diazo Transfer Reaction.

Clicks: 145
ID: 61225
2019
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Abstract
The synthesis of 1,2,3-triazoles with sulfur-based side chain has been accessed with the metal-free annulation reactions of readily available β-thiolated enaminones and tosyl hydrazine. By these reactions with water as the only medium, a broad array of 5-thiolated 1,2,3-triazoles have been synthesized with generally good to excellent yields. Except using TMEDA (N,N,N',N'-tetramethylethylenediamine) as the only base promoter, not any other catalyst or additive is required, thus providing an efficient and environmentally benign methods for useful 1,2,3-triazole synthesis.
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deng2019inwaterthe Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Deng, Leiling;Cao, Xiaoji;Liu, Yunyun;Wan, Jie-Ping;
Journal The Journal of organic chemistry
Year 2019
DOI
10.1021/acs.joc.9b01817
URL
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