Synthesis of (E,E)-Dienones and (E,E)-Dienals via Palladium-Catalyzed γ,δ-Dehydrogenation of Enones and Enals.

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ID: 58784
2019
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Abstract
A new strategy for the synthesis of conjugated (E,E)-dienones and (E,E)-dienals via a palladium-catalyzed aerobic γ,δ-dehydrogenation of enones and enals has been developed. The method can be employed in the direct and efficient synthesis of various (E,E)-dienones and (E,E)-dienals, including non-substituted α-, β-, and γ- and/or δ-substituted (E,E)-dienones and (E,E)-dienals. The protocol is featured by the ready accessibility and elaboration of the starting materials, good functional group compatibility, and mild reaction conditions. Furthermore, the reaction is of complete E,E-stereoselectivity and uses molecular oxygen as the sole clean oxidant.
Reference Key
pan2019synthesisiscience Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Pan, Gao-Fei;Zhang, Xing-Long;Zhu, Xue-Qing;Guo, Rui-Li;Wang, Yong-Qiang;
Journal iScience
Year 2019
DOI
S2589-0042(19)30365-7
URL
Keywords
organic synthesis catalysis chemical compounds in materials science

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