Intramolecular oxidative cyclization of N-(2,2,2-trifluoro-1-(phenylimino)ethyl)benzimidamide.

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ID: 58117
2019
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Abstract
A fast and convenient method for synthesis of 1,3-diaryl-5-(trifluoromethyl)-1H-1,2,4-triazole compounds has been described via intramolecular oxidative cyclization of the N-(2,2,2-trifluoro-1-(arylimino)ethyl)benzimidamide intermediates by I/KI in excellent yields without any purification. N-(2,2,2-Trifluoro-1-(arylimino)ethyl)benzimidamide intermediates which are used in this project have been synthesized from the reaction of N-aryl-2,2,2-trifluoroacetimidoyl chlorides and benzamide hydrochloride derivatives at room temperature for the first time.
Reference Key
kazemi2019intramolecularmolecular Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Kazemi, Elham;Darehkordi, Ali;
Journal Molecular diversity
Year 2019
DOI
10.1007/s11030-019-09995-8
URL
Keywords
1,2,4-triazoles 2,2,2-trifluoro acetimidoyl chloride amidine oxidative cyclization

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