One-Pot Synthesis of Amide-Functional Main-Chain Polybenzoxazine Precursors.

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ID: 57137
2019
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Abstract
Main-chain polybenzoxazines containing amide linkages were successfully prepared in one pot. Three different polymers were synthesized by reacting 3,4-dihydrocoumarine (DHC) and paraformaldehyde with 1,3-diaminopropane or 1,6-diaminohexane or Jeffamine ED-900. The one-pot reaction proceeded through the combination of the ring-opening of DHC with amines, and subsequent Mannich and ring-closure reactions occurring in a cascading manner. The obtained polymer from Jeffamine exhibited good film-forming properties, and free-standing flexible films were easily solvent- casted on Teflon plates. All polymeric precursors were characterized by spectroscopic analysis, and their curing behavior and thermal stability were investigated by differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA).
Reference Key
durukan2019onepotpolymers Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Durukan, Canan;Kiskan, Baris;Yagci, Yusuf;
Journal Polymers
Year 2019
DOI
E679
URL
Keywords
benzoxazine dihydrocoumarine polyamide polybenzoxazine ring-opening polymerization sba-15 nanostructured silica 3 analgesia 5 crotoxin 2 hypernociception 6 neuropathic pain 1 partial sciatic nerve ligation 4 security smart grid integrity communication architecture distribution system

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