Crystal structure of poly[tetra-μ-chlorido-tetra-chlorido-bis-(μ-4,4'-bi-1,2,4-triazole-κ::)(μ-4,4'-bi-1,2,4-triazole-κ:)tetra-copper(II)].

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ID: 4771
2019
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Abstract
The title Cu-chloride coordination polymer with the 4,4'-bi-1,2,4-triazole ligand (btr), [CuCl(CHN)] , crystallizes in the non-centrosymmetric ortho-rhom-bic space group F2. The two independent Cu cations adopt distorted square-pyramidal geometries with {ClN+Cl} coordination polyhedra. The metal atoms are bridged by -Cl anions forming left- and right-handed helical chains of sequence [-(-Cl)CuCl-] along the axis direction. In the perpendicular directions, the btr ligands act in - and - coordination modes in a 2:3 ratio. The -btr bridges connect neighboring helices of the same handedness, whereas the -btr ligands link the helices of opposite handedness, leading to a racemic three-dimensional framework. The structure is consolidated by weak C-H⋯Cl and C-H⋯N inter-actions.
Reference Key
domasevitch2019crystalacta Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Domasevitch, Kostiantyn V;Lysenko, Andrey B;
Journal acta crystallographica section e: crystallographic communications
Year 2019
DOI
10.1107/S2056989019005516
URL
Keywords Keywords not found

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