NH3 Synthesis from 1.0 vol% Nitric Oxide Gas via Direct Electrocatalytic Reduction

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ID: 322742
2026
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Abstract
Abstract Ammonia is a promising zero-carbon energy carrier; however, its conventional production is energy-intensive and dependent on fossil fuels. The electrochemical reduction of nitric oxide offers a sustainable alternative for ammonia synthesis while simultaneously mitigating nitrogen oxide pollutants. In this study, a solid polymer electrolyte cell equipped with an anion-exchange membrane was employed to improve nitric oxide mass-transfer and suppress the competing hydrogen evolution reaction by establishing a localized alkaline environment. Using a copper catalyst supported on carbon, ammonia was successfully produced with a Faraday efficiency of 22%. The introduction of platinum as a secondary metal further enhanced the catalytic performance. Under continuous electrolysis at a current density of −50 mA cm−2, the bimetallic copper–platinum catalyst achieved an ammonia formation rate of 2.2 mg h−1 cm−2, a Faraday efficiency of 34%, and a nitric oxide-to-ammonia conversion of 23%. These results demonstrated an effective strategy for continuous ammonia electrosynthesis from dilute nitric oxide streams and suggested a promising approach for utilizing low-concentration nitrogen oxide sources.
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openalex_W7171658168 Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Kaito Oya, Shoji Iguchi, Shimpei Naniwa, Kentaro Teramura
Journal bulletin of the chemical society of japan
Year 2026
DOI
10.1093/bulcsj/uoag108
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