Founding Strategic Bases for the Total Synthesis of Naphthocyclinones: Design and Preparation of an Acceptor Unit and Stereoselective Construction of the Bicyclic Framework
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ID: 322321
2026
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Abstract
Abstract Synthetic study on the naphthocyclinones is described, focusing on the design of a viable acceptor unit for 1,4-addition to develop feasible synthetic routes. Valuable insights have been uncovered, concerning the unique reactivity of hydroquinone and the photo-lability of naphthoquinone during their preparation. Furthermore, the acceptor unit was employed for studying the construction of the bicyclo[3.2.1]octadienone core by the planned key reactions, Rh-mediated stereoselective 1,4-addition and thiolate-mediated reductive cyclization. The knowledge provided a firm basis for our preceding total synthesis that was recently reported.
| Reference Key |
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| Authors | Yoshio Ando, Nozomi Tanaka, Mark M. Maturi, Ken Ohmori, Keisuke Suzuki |
| Journal | bulletin of the chemical society of japan |
| Year | 2026 |
| DOI |
10.1093/bulcsj/uoag105
|
| URL | |
| Keywords | Keywords not found |
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