Synthesis of N,N'-diglycosylated isoindigos.

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ID: 31322
2013
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Abstract
The first N,N'-diglycosylated isoindigos were prepared by P(NEt(2))(3)-mediated dimerization of acetyl protected N-glycosyl-5-alkylisatins. Subsequent deacetylation yielded the corresponding deprotected N,N'-diglycosylated isoindigos. Isatine-N-glycosides containing an unsubstituted or alkyl-substituted heterocyclic moiety and β-D-manno- and β-L-rhamno configured carbohydrate substituents were successfully transformed into the corresponding isoindigos. In contrast, isatins with β-D-gluco- or β-D-xylo configured substituents failed to give the desired products.
Reference Key
kleeblatt2013synthesisorganic Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Kleeblatt, Dennis;Siyo, Baraa;Hein, Martin;Iaroshenko, Viktor O;Iqbal, Jamshed;Villinger, Alexander;Langer, Peter;
Journal Organic & biomolecular chemistry
Year 2013
DOI
10.1039/c2ob25866h
URL
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