Preparation of Esters of Carboxylic and Phosphoric Acid via Quaternary Phosphonium Salts

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ID: 303838
1967
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Abstract
Abstract When n-valeric acid was treated with allyl diethyl phosphite and diethyl azodicarboxylate, allyl valeriate and diethyl N-(diethyl)phosphoryl hydrazodicarboxylate were obtained in good yields. Similarly ethyl benzoate was obtained in a nearly quantitative yield by the reaction of benzoic acid with triethyl phosphite and diethyl azodicarboxylate. The reaction of carboxylic acid with triphenyl phosphine and diethyl azodicarboxylate in the presence of an alcohol resulted in the formation of the corresponding esters of the carboxylic acid, triphenyl phosphine oxide, and diethyl hydrazodicarboxylate. The mechanisms of these reactions are also discussed.
Reference Key
openalex_W2012182437 Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Oyo Mitsunobu, Masaaki Yamada
Journal bulletin of the chemical society of japan
Year 1967
DOI
10.1246/bcsj.40.2380
URL
https://doi.org/10.1246/bcsj.40.2380
Keywords Keywords not found

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