Thermal and EPR spectroscopic studies of novel coordination compound trans-bis(acesulfamato)tetraaquazinc(II) with Mn(II) impurity.

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ID: 2841
2011
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Abstract
The thermogravimetric analysis (TGA) and electron paramagnetic resonance (EPR) studies of powder and single crystals of bis(acesulfamato)tetraaquazinc(II), Zn(acs)(2)(H(2)O)(4), a novel coordination compound, are carried out. Previously synthesized bis(acesulfamato) tetraaquamanganese(II), Mn(acs)(2)(H(2)O)(4), is included into the host in trace amount as a paramagnetic probe for EPR analysis. Single crystal EPR spectra at room temperature are resolved and discussed. Low temperature EPR spectra down to 90K do not show remarkable change. At higher temperatures, however, the TGA and EPR spectra show changes around 335 K and 395 K; the causes and the mechanisms of changes are discussed.
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fidan2011thermalspectrochimica Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Fidan, M;Icbudak, H;Tapramaz, R;Sahin, Y;
Journal spectrochimica acta part a, molecular and biomolecular spectroscopy
Year 2011
DOI
10.1016/j.saa.2010.12.028
URL
Keywords Keywords not found

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