Synthesis of Boron-Doped Carbon Nanomaterial.

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ID: 276553
2023
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Abstract
A new method for the synthesis of boron-doped carbon nanomaterial (B-carbon nanomaterial) has been developed. First, graphene was synthesized using the template method. Magnesium oxide was used as the template that was dissolved with hydrochloric acid after the graphene deposition on its surface. The specific surface area of the synthesized graphene was equal to 1300 m/g. The suggested method includes the graphene synthesis via the template method, followed by the deposition of an additional graphene layer doped with boron in an autoclave at 650 °C, using a mixture of phenylboronic acid, acetone, and ethanol. After this carbonization procedure, the mass of the graphene sample increased by 70%. The properties of B-carbon nanomaterial were studied using X-ray photoelectron spectroscopy (XPS), high-resolution transmission electron microscopy (HRTEM), Raman spectroscopy, and adsorption-desorption techniques. The deposition of an additional graphene layer doped with boron led to an increase of the graphene layer thickness from 2-4 to 3-8 monolayers, and a decrease of the specific surface area from 1300 to 800 m/g. The boron concentration in B-carbon nanomaterial determined by different physical methods was about 4 wt.%.
Reference Key
chesnokov2023synthesismaterials Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Chesnokov, Vladimir V;Prosvirin, Igor P;Gerasimov, Evgeny Yu;Chichkan, Aleksandra S;
Journal Materials (Basel, Switzerland)
Year 2023
DOI
1986
URL
Keywords
synthesis doping graphene boron

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