Solid-solid interactions—IV: Thorium nitrate-urea complexes
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ID: 270148
1966
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Abstract
Using the technique of solid-solid interaction and from solution the following series of complexes were obtained: [Th(NO3)4(Urea)2(H2O)2], [Th(NO3)4(urea)3(H2O)1], [Th(Urea)6(H2O)2](NO3)4, [Th(NO3)2(Urea)6](NO3)2, [Th(NO3)4(Urea)2(H2O)1] and [Th(Urea)8](NO3)4. In all cases urea exhibited oxygen-to-thorium bonding. A reasonable argument for octacoordination could be made for all of the complexes except [Th(NO3)4(Urea)2(H2O)1]. Finally, the deleterious effects upon the infra-red spectra are noted owing to KBr-complex interactions occurring in the solid state in KBr pellets.
| Reference Key |
carfagno1966journalsolid-solid
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| Authors | P.S. Gentile,L.S. Campisi,P. Carfagno;P.S. Gentile;L.S. Campisi;P. Carfagno; |
| Journal | Journal of Inorganic and Nuclear Chemistry |
| Year | 1966 |
| DOI |
10.1016/0022-1902(66)80439-6
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