synthesis and surface thermodynamic functions of camoo4 nanocakes
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ID: 259706
2015
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Abstract
CaMoO4 nanocakes with uniform size and morphology were prepared on a large scale via a room temperature reverse-microemulsion method. The products were characterized in detail by X-ray powder diffraction, field-emission scanning electron microscopy, transmission electron microscopy, and high-resolution transmission electron microscopy. By establishing the relations between the thermodynamic functions of nano-CaMoO4 and bulk-CaMoO4 reaction systems, the equations for calculating the surface thermodynamic functions of nano-CaMoO4 were derived. Then, combined with in-situ microcalorimetry, the molar surface enthalpy, molar surface Gibbs free energy, and molar surface entropy of the prepared CaMoO4 nanocakes at 298.15 K were successfully obtained as (19.674 ± 0.017) kJ·mol−1, (619.704 ± 0.016) J·mol−1, and (63.908 ± 0.057) J·mol−1·K−1, respectively.
| Reference Key |
li2015entropysynthesis
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|---|---|
| Authors | ;Xingxing Li;Gaochao Fan;Zaiyin Huang |
| Journal | European journal of medicinal chemistry |
| Year | 2015 |
| DOI |
10.3390/e17052741
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