caracterização térmica de fios de poliaramida characterization of aramid yarns
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ID: 256169
2007
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Abstract
A poliaramida (aramida) é um polímero de alto desempenho, cujas principais características são a elevada tenacidade, baixo alongamento e resistência ao calor. Devido ao desconhecimento do mercado em geral a respeito de materiais têxteis, metodologia de ensaios e a nomenclatura utilizada nesta família de materiais, invariavelmente ocorrem erros na escolha da qualidade do produto a adquirir. O uso de equipamentos inadequados para caracterização deste material pode levar a erros de interpretação. Este trabalho visa a melhor informar sobre este mercado, e discutir análises já realizadas. O gráfico tensão x deformação da poliaramida obtido em equipamento e garras corretas é linear, o que não ocorre se o equipamento de tração equipado com garras não for preparado para ensaios de tração de fios têxteis. Em análise termogravimétrica, verificou-se que a taxa de elevação de temperatura mais adequada é de aproximadamente 3 °C/min. A degradação da poliaramida se inicia a aproximadamente 510 °C, pela decomposição térmica das ligações simples, seguida da decomposição térmica dos anéis aromáticos a aproximadamente 525 ºC, sendo que a temperatura de degradação térmica completa ocorre a cerca de 575 °C.
Polyaramid (aramid) is a high performance polymer, whose main characteristics are its high tenacity, low elongation and good heat resistance. Owing to the lack of familiarity of the market with textile materials, methods of analysis and the nomenclature used for this family of materials, errors in the choice of the product quality are common. The inadequate use of equipment in the characterization of this material may lead to errors of interpretation. This work aims to inform about this market, and discuss results of previous analyses. A stress x strain graph of polyaramid is linear if obtained with adequate equipment and fixtures, which is not the case if the equipment and fixtures are not suitable for textile yarns. In the thermo-gravimetric analysis, the best heating rate was approximately 3 °C/min. Degradation started at 510 ºC with breaking of single bonds, which was followed by degradation of aromatic rings at 525 ºC. Complete thermal degradation occurred at 575 °C.
Polyaramid (aramid) is a high performance polymer, whose main characteristics are its high tenacity, low elongation and good heat resistance. Owing to the lack of familiarity of the market with textile materials, methods of analysis and the nomenclature used for this family of materials, errors in the choice of the product quality are common. The inadequate use of equipment in the characterization of this material may lead to errors of interpretation. This work aims to inform about this market, and discuss results of previous analyses. A stress x strain graph of polyaramid is linear if obtained with adequate equipment and fixtures, which is not the case if the equipment and fixtures are not suitable for textile yarns. In the thermo-gravimetric analysis, the best heating rate was approximately 3 °C/min. Degradation started at 510 ºC with breaking of single bonds, which was followed by degradation of aromatic rings at 525 ºC. Complete thermal degradation occurred at 575 °C.
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boukouvalas2007polmeroscaracterizao
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| Authors | ;Nicolas T. Boukouvalas;Hélio Wiebeck |
| Journal | journal of the chemical society, perkin transactions 1 |
| Year | 2007 |
| DOI |
10.1590/S0104-14282007000400006
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