a mild catalytic oxidation system: fepcotf/h2o2 applied for cyclohexene dihydroxylation

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ID: 253190
2015
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Abstract
Iron (III) phthalocyanine complexes were employed for the first time as a mild and efficient Lewis acid catalyst in the selective oxidation of cyclohexene to cyclohexane-1,2-diol. It was found that the catalyst FePcOTf shown excellent conversion and moderate selectivity relative to other iron (III) phthalocyanine complexes. The optimum conditions of the oxidation reaction catalyzed by FePcOTf/H2O2 have been researched in this paper. Iron (III) phthalocyanine triflate (1 mol %) as catalyst, hydrogen peroxide as oxidant, methanol as solvent, and a mole ratio of substrate and oxidant (H2O2) of 1:1 were used for achieving moderate yields of 1,2-diols under reflux conditions after eight hours.
Reference Key
zhou2015moleculesa Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors Baocheng Zhou, Wenxing Chen
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Journal Journal of ethnopharmacology
Year 2015
DOI
10.3390/molecules20058429
URL
http://www.mdpi.com/1420-3049/20/5/8429
Keywords Keywords not found

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