mechanical and morphological properties of poly-3-hydroxybutyrate/poly(butyleneadipate-co-terephthalate)/layered double hydroxide nanocomposites
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ID: 250643
2013
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Abstract
Nanocomposites of poly-3-hydroxybutyrate/poly(butyleneadipate-co-terephthalate)/layered double hydroxide (PHB/PBAT/LDH) were prepared from a binary blend of PHB/PBAT and stearate-Zn3Al LDH via a solution casting method using chloroform as solvent in this study. The pristine Zn3Al LDH was synthesized from nitrate salts solution at pH 7 by using coprecipitation technique and then was modified by stearate anions surfactant via ion exchange reaction. As a result, the basal spacing of the LDH was increased from 8.77 to 24.94 Å after the modification. Intercalated nanocomposites were formed due to the presence of diffraction peak in XRD diffractograms. The infrared spectrum of stearate-Zn3Al LDH exhibited the existence of stearate anions in the synthesized Zn3Al LDH. Mechanical properties with 2 wt% stearate-Zn3Al LDH loading nanocomposites showed 56 wt% improvements in elongation at break compared to those of the blend.
| Reference Key |
pak2013journalmechanical
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|---|---|
| Authors | ;Yen Leng Pak;Mansor Bin Ahmad;Kamyar Shameli;Wan Md Zin Wan Yunus;Nor Azowa Ibrahim;Norhazlin Zainuddin |
| Journal | reproductive biology and endocrinology |
| Year | 2013 |
| DOI |
10.1155/2013/621097
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| URL | |
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