the reaction mechanism of acetaldehyde ammoximation to its oxime in the ts-1/h2o2 system
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2016
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Abstract
A qualitative analysis for the ammoximation of acetaldehyde to its oxime in the TS-1(Titanium Silicalite-1)/H2O2 system was investigated using an in situ infrared spectrometer (ReactIR15). NH3 is first oxidized to NH2OH by TS-1/H2O2; then, CH3CH=NOH forms after NH2OH reacts with CH3CHO. That means the intermediate of this reaction is NH2OH instead of CH3CH=NH. Experiments have been conducted to verify the mechanism, and the results are in good agreement with the infrared findings.
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meng2016catalyststhe
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| Authors | ;Chaoqun Meng;Suohe Yang;Guangxiang He;Guohua Luo;Xin Xu;Haibo Jin |
| Journal | journal of essential oil research |
| Year | 2016 |
| DOI |
10.3390/catal6070109
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