1,4,9,12-tetramethoxy-14-octyl-5,8-dihydrodiindolo[3,2-b;2′,3′-h]carbazole with an unknown solvent

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ID: 247449
2017
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Abstract
The title compound, 2C36H39N3O4·H2O, is a linear π-conjugated ladder oligomer with an alkyl chain on the central nitrogen atom. This diindolocarbazole, prepared via a twofold Cadogan reaction, adopts a sligthly convex shape, anti to the disordered octyl group. The unit cell contains nine molecules of the title compound and half a water molecule per main molecule. The water molecule forms hydrogen bridges, connecting the carbazole-NH and methoxy groups of different molecules. The crystal contains solvent molecules which are located in a channel parallel to the c axis. It was not possible to determine the position and nature of the solvent (a mixure of choroform, n-pentane and DMSO). The SQUEEZE [Spek (2015). Acta Cryst. C71, 9–18] option of PLATON was used to model the missing electron density. The given chemical formula and other crystal data do not take into account these solvent molecules.
Reference Key
wrobel2017iucrdata1,4,9,12-tetramethoxy-14-octyl-5,8-dihydrodiindolo[3,2-b;2,3-h]carbazole Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors ;Norma Wrobel;Bernhard Witulski;Dieter Schollmeyer;Heiner Detert
Journal lecture notes in civil engineering
Year 2017
DOI
10.1107/S241431461700462X
URL
http://scripts.iucr.org/cgi-bin/paper?S241431461700462X
Keywords
crystal structure hydrogen bondingcrystallography

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