síntese da fenitoína assistida por micro-ondas: proposta de aula prática para alunos de graduação
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ID: 247377
2012
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Abstract
Microwave synthesis is considered a breakthrough in the field of chemistry due to its benefits over conventional heating methods. We describe, for the first time, the total synthesis of phenytoin adapted for a microwave reactor, proposed as an experiment for undergraduate courses. When carried out with microwaves, the synthetic route provided phenytoin in 6 min and 30 s, while for conventional heating the total time was 170 min. The experiment also involves rapid identification of compounds by TLC, ¹H NMR, FT-IR and melting points determination.
| Reference Key |
konrath2012qumicasntese
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|---|---|
| Authors | ;Eduardo L. Konrath;Maristela Piedade;Vera Lucia Eifler-Lima |
| Journal | greece and rome |
| Year | 2012 |
| DOI |
10.1590/S0100-40422012000900033
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