redetermination of catena-poly[[chloridolead(ii)]-μ2-chlorido-di-μ2-thiourea-κ4s:s] at 100 k
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ID: 243116
2016
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Abstract
Although the structure rerefinement (CCD data at 100 K) of the polymeric lead(II) thiourea complex, [PbCl2·2tu]n where (tu = SCN2H4), basically confirmed the previous study based on integrated Weissenberg data recorded at room temperature [Nardelli & Fava (1959). Acta Cryst. 12, 727–732]; all atomic positions could be determined with significantly higher precision and accuracy. In addition, all H atoms could be located from difference maps, revealing details of the hydrogen-bonding scheme.
| Reference Key |
zouihri2016iucrdataredetermination
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|---|---|
| Authors | ;Hafid Zouihri;Khalid Yamni;Youssef Messouss;Najib Tijani;Lahcen Messaoudi |
| Journal | lecture notes in civil engineering |
| Year | 2016 |
| DOI |
10.1107/S2414314616017454
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