high-performance and simply-synthesized ladder-like structured methacrylate siloxane hybrid material for flexible hard coating
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ID: 241258
2018
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Abstract
A high performance ladder-like structured methacrylate siloxane hybrid material (LMSH) was fabricated via simple hydrolytic sol–gel reaction, followed by free-radical polymerization. A structurally ordered siloxane backbone, the ladder-like structure, which is an essential factor for high performance, could be achieved by a short period of sol–gel reaction in only 4 h. This results in superior optical (Transmittance > 90% at 550 nm), thermal (T5 wt % decomposition > 400 ℃ ), mechanical properties(elastic recovery = 0.86, hardness = 0.6 GPa) compared to the random- and even commercialized cage-structured silsesquioxane, which also has ordered structure. It was investigated that the fabricated ladder-like structured MSH showed the highest overall density of organic/inorganic co-networks that are originated from highly ordered siloxane network, along with high conversion rate of polymerizable methacrylate groups. Our findings suggest a potential of the ladder-like structured MSH as a powerful alternative for the methacrylate polysilsesquioxane, which can be applied to thermally stable and flexible optical coatings, even with an easier and simpler preparation process.
| Reference Key |
kim2018polymershigh-performance
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|---|---|
| Authors | ;Yun Hyeok Kim;Gwang-Mun Choi;Jin Gyu Bae;Yong Ho Kim;Byeong-Soo Bae |
| Journal | Journal of Fluorescence |
| Year | 2018 |
| DOI |
10.3390/polym10040449
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| URL | |
| Keywords | Keywords not found |
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