synthesis, characterization and thermal analysis of a new acetic acid (2-hydroxy-benzylidene)-hydrazide and its complexes with hg(ii) and pd(ii)
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ID: 240569
2011
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Abstract
The new complexes have been synthesized by the reaction of Hg(II) and Pd(II) with acetic acid(2-hydroxy-benzylidene)- hydrazide (L). These new complexes were characterized by elemental analysis, IR, H NMR spectroscopy and UV spectral techniques. The changes observed between the FT-IR, H NMR and UV-Vis spectra of the ligands and of the complexes allowed us to establish the coordination mode of the metal in complexes. Thermal properties, TG-DTA of these complexes were studied. TG- DTA and other analytical methods have been applied to the investigation of the thermal behavior and structure of the compounds [M(L)2]Cl2 M= Hg, Pd. Thermal decomposition of these compounds is multi-stage processes.
| Reference Key |
sahebalzamani2011e-journalsynthesis,
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| Authors | ;Hajar Sahebalzamani;Shahriare Ghammamy;Shaghayegh Dexhkam;Alireza Hemati Moghadam;Farhod Siavoshifar |
| Journal | Journal of pharmaceutical and biomedical analysis |
| Year | 2011 |
| DOI |
10.1155/2011/270304
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