(4z,5e,9e,10z)-n4,n5,n9,n10-tetrakis(2,6-diisopropylphenyl)pyrene-4,5,9,10-tetraimine

Clicks: 203
ID: 230088
2016
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Abstract
The title molecule, C64H74N4, consists of a pyrene backbone with imine moieties located on the 4-, 5-, 9-, and 10-positions of the ring system. The aryl groups on these imines are sterically bulky 2,6-diisopropylphenyl units. As a consequence, the backbone itself is twisted, with an angle of 15.29 (6)° between the mean planes (r.m.s. deviations = 0.006 and 0.009 Å) of the phenyl units. The N=C—C=N units are significantly twisted and feature torsion angles of −48.8 (2) and −46.3 (3)°. The non-planarity of the backbone and short C—N distances [ranging from 1.281 (2) to 1.285 (2) Å] indicate the lack of conjugation in the molecule and double-bond nature of the imines. Weak intramolecular and intermolecular C—H...π interactions are observed.
Reference Key
williams2016iucrdata(4z,5e,9e,10z)-n4,n5,n9,n10-tetrakis(2,6-diisopropylphenyl)pyrene-4,5,9,10-tetraimine Use this key to autocite in the manuscript while using SciMatic Manuscript Manager or Thesis Manager
Authors ;Owen M. Williams;Alan H. Cowley
Journal lecture notes in civil engineering
Year 2016
DOI
10.1107/S2414314616004843
URL
http://scripts.iucr.org/cgi-bin/paper?S2414314616004843
Keywords
crystal structure pyrene

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