synthesis and characterization of nanocrystalline ysz powder by smoldering combustion synthesis
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ID: 226097
2006
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Abstract
Nanocrystalline yttria-stabilized zirconia (YSZ) powders with
8 mol% Y2O3 have been produced using
smoldering combustion synthesis with glycine as fuel and nitrate
as oxidizer. The YSZ powders prepared by using different glycine
to nitrate ratios (0.20–1.0) have been characterized by X-ray
diffraction (crystallite size), thermogravimetry, infrared
spectroscopy, surface area analysis, transmission electron
microscopy, and dilatometry to determine the parameters giving the
powder the best properties when it comes to densification
properties. The influence of calcination temperature on
crystallite size, surface area, and carbonate species remaining
from the smoldering combustion reaction has been studied
especially for the G/N ratio of 0.23 to reveal the
optimal synthesis conditions. A G/N ratio of 0.23 and
calcination in the range 650–900ºC in oxygen flow gave
high quality powder with a crystallite size less than 10 nm.
Densities of sintered bodies exhibit an increase for calcination
temperatures above 600ºC, where most of the residual
carbonate species has been removed.
| Reference Key |
kaus2006journalsynthesis
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|---|---|
| Authors | ;Ingeborg Kaus;Paul Inge Dahl;Johann Mastin;Tor Grande;Mari-Ann Einarsrud |
| Journal | reproductive biology and endocrinology |
| Year | 2006 |
| DOI |
10.1155/JNM/2006/49283
|
| URL | |
| Keywords |
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