preparation of graphene/tio2 composite nanomaterials and its photocatalytic performance for the degradation of 2,4-dichlorophenoxyacetic acid
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2016
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Abstract
The graphene (GR) was prepared by an improved electrochemical stripping method using a high-purity graphite rod as raw material and high temperature heat reduction in hydrogen atmosphere, and the graphene/TiO2 (GR/TiO2) composite nanomaterials were manufactured by the method of sol-gel and high temperature crystallization in hydrogen atmosphere using butyl titanate and electrolysis graphene as precursors. The physical and chemical properties of the composites had been characterized by using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), UV-Vis spectrophotometer (UV-Vis), scanning electron microscopy (SEM), Transmission Electron Microscope (TEM), and specific surface area (SSA) by BET method. The photocatalytic properties of GR/TiO2 composites nanomaterials in anoxic water were studied by using 2,4-dichlorophenoxyacetic acid (2,4-D) as probe. The results showed that graphite was well intercalated and peeled by a facile electrolysis method in different electric field environment; a well dispersed and rings structure of graphene was prepared by coupling ultrasound-assisted changing voltage electrochemical stripping technology. The as-prepared GR/TiO2 composites had good performance for the photocatalytic degradation of 2,4-D in anoxic water; the chlorines were removed from benzene ring; the middle products of dichlorophenol, chlorophenol, phloroglucinol, and so forth were produced from the photocatalytic redox reaction of 2,4-D in anoxic water; parts of 2,4-D were decomposed completely, and CO2 and H2O were produced.
| Reference Key |
huang2016journalpreparation
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|---|---|
| Authors | ;Donggen Huang;Tianzi Yang;Zhuanghong Mo;Qin Guo;Shuiqing Quan;Cui Luo;Lei Liu |
| Journal | reproductive biology and endocrinology |
| Year | 2016 |
| DOI |
10.1155/2016/5858906
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| URL | |
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