synthesis of 1-methyl-3-oxo-7-oxabicyclo[2.2.1]hept-5-ene-2-carboxylic acid methyl ester
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ID: 209757
2005
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Abstract
A simple and efficient method for the preparation of 1-methyl-3-oxo-7- oxabicyclo[2.2.1]hept-5-en-2-carboxylic acid methyl ester (1) is described. The first step is a highly regioselective Diels-Alder reaction between 2-methylfuran and methyl-3-bromo- propiolate. A remarkably difficult ketal hydrolysis reaction was effected by treatment with HCl, a simple reagent that was shown to be more efficient, in this case, than commonly used more elaborate methods.
| Reference Key |
silva2005moleculessynthesis
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|---|---|
| Authors | ;Gil Valdo José da Silva;Adilson Beatriz;Mauricio Gomes Constantino;Valquiria Aragao |
| Journal | Journal of ethnopharmacology |
| Year | 2005 |
| DOI |
10.3390/10111413
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| URL | |
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