efficient dehydration of fructose to 5-hydroxy-methylfurfural catalyzed by heteropolyacid salts
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ID: 200908
2016
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Abstract
5-Hydroxymethylfurfural (5-HMF), which is derived from numerous industrial biomass resources, has attracted attention in recent years due to its potential as a building block. In this paper, a range of heteropolyacid salts had been investigated for the dehydration of fructose to 5-HMF. CePW12O40 demonstrated the best catalytic activity. Effects of fructose concentration, reaction temperature and reaction time on 5-HMF yield were investigated and optimised through a central composite design and response surface methodology. The optimal 5-HMF yield was 99.40% under the optimized reaction conditions of 5.48 mg/mL fructose loading, 158 °C temperature and 164 min reaction time. A kinetic analysis of the fructose conversion was also performed, and the activation energy and pre-exponential factor were obtained.
| Reference Key |
song2016catalystsefficient
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|---|---|
| Authors | ;Yanlei Song;Xincheng Wang;Yongshui Qu;Chongpin Huang;Yingxia Li;Biaohua Chen |
| Journal | journal of essential oil research |
| Year | 2016 |
| DOI |
10.3390/catal6040049
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