quantitative 1h-nmr method for the determination of tadalafil in bulk drugs and its tablets
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ID: 193636
2015
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Abstract
A simple, rapid, accurate, and selective quantitative nuclear magnetic resonance method for the determination of tadalafil in bulk drugs and its tablets was established and evaluated. Spectra were obtained in dimethylsulfoxide-d6 using 2,4-dinitrotoluene as the internal standard. In this study, the method’s linearity, range, limit of quantification, stability, precision, and accuracy were validated. The results were consistent with those obtained from high-performance liquid chromatography analysis. Thus, the proposed method is a useful and practical tool for the determination of tadalafil in bulk drugs and its tablets.
| Reference Key |
yang2015moleculesquantitative
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|---|---|
| Authors | ;Qingyun Yang;Hui Qiu;Wei Guo;Dongmei Wang;Xingning Zhou;Dan Xue;Jinlan Zhang;Song Wu;Yinghong Wang |
| Journal | Journal of ethnopharmacology |
| Year | 2015 |
| DOI |
10.3390/molecules200712114
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